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My interests lie in the application of novel electron microscopy
techniques to the analysis of defects and interfaces, particularly in
semiconductors, to clarify microstructure/property relationships. My
present research includes the development of new materials for field
emission displays, and studies of the role of defects in GaN
light-emitting structures. In the latter, we have used transmission
electron microscopy to analyse threading defects including
dislocations, nanopipes and inversion domains. We have demonstrated,
for the first time, that electron holography can be used to profile
piezoelectric fields across InGaN quantum wells and around
dislocations, and have used cathodoluminescence in a field-emission
scanning electron microscope to examine the effects of individual
threading defects on light emission.
Some images from recently published work
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Images from a GaN (0001) sample with a 1.5 nm In0.28Ga0.72N
quantum well buried 50 nm below the top surface.
The
left hand micrograph is a tranmission electron micrscope image from a plan
view sample which has been slightly tilted to reveal a funnel-shaped pit and
some threading edge dislocations. The right hand pair of images are
from a different area, (a) shows a TEM image and (b) shows a corresponding
cathodoluminescence map in the quantum well emission, taken at 8K in a
scanning electron microscope. The CL map shows that pits and threading
dislocations (positions marked) act as nonradiative recombination centres.
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Electron holography results: the micrograph on the left shows
a holographic image from an edge dislocation in GaN viewed near end-on (in
the centre of the outlined box). The graph on the right shows that the
crystal potential is reduced within a few nm of the core consistent with the
core being negatively charged. |
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